MARC record from Internet Archive

LEADER: 06609cam 22004934a 4500
001 ocm44841582
003 OCoLC
005 20200518202123.0
008 000808s2000 caua b 001 0 eng
010 $a 00063434
040 $aDLC$beng$cDLC$dC#P$dUKM$dBAKER$dBTCTA$dYDXCP$dDEBBG$dTULIB$dVXI$dOCLCF$dIG#$dIOO$dOCLCQ$dSNN$dUKMGB$dOCLCQ
015 $aGBA335793$2bnb
016 7 $a008833180$2Uk
020 $a1891389181$q(acid-free paper)
020 $a9781891389184$q(acid-free paper)
035 $a(OCoLC)44841582
042 $apcc
050 00 $aQD96.N8$bR63 2000
082 00 $a543/.0877$221
084 $aCHE 244f$2stub
084 $aVG 9200$2rvk
100 1 $aRoberts, John D.,$d1918-2016.
245 10 $aABCs of FT-NMR /$cJohn D. Roberts.
260 $aSausalito, Calif. :$bUniversity Science Books,$c℗♭2000.
300 $axiii, 322 pages :$billustrations ;$c26 cm
336 $atext$btxt$2rdacontent
337 $aunmediated$bn$2rdamedia
338 $avolume$bnc$2rdacarrier
504 $aIncludes bibliographical references and index.
505 00 $g1.$tSome NMR Basics --$g1-1.$tWhat Should You Know Already --$g1-2.$tQualitative Quantum-Mechanical View of NMR --$g2.$tElectromagnetic Basics of NMR --$g2-1.$tPrecession, Phase and Excitation --$g2-2.$tRelaxation --$g2-3.$tDetermination of T[subscript 2]. Echo trains --$g2-4.$tDetermination of T[subscript 1]. Inversion Recovery --$g2-5.$tMore on the 90[degree] Pulse --$g3.$tHow do We Perform the NMR Fourier Transform? --$g3-1.$tBasics of the Fourier Transform --$g3-2.$tApplying the Fourier Transform --$g4.$tBloch Equations. Calculating What Happens in NMR Experiments --$g4-1.$tInitial Steps. Relaxation --$g4-2.$tNext Step. Taking Into Account the B[subscript 1] Power Input --$g4-3.$tNMR at Equilibrium. Slow-Passage Conditions --$g4-4.$tNMR Under Non-Equilibrium Conditions. Initial Conditions --$g4-5.$tNumerical Integration Procedure for the Bloch Equations --$g4-6.$tMore on CW-NMR --$g4-7.$tResolution in CW Spectra --$g4-8.$tRapid-Scan (Correlation) Spectroscopy. The Inverse Fourier Transform --$g4-9.$tCW Adiabatic Rapid-Passage Dispersion-Mode Spectra --$g5.$tNMR Fourier Transform and Its Problems --$g5-1.$tRise of [superscript 13]C NMR and the Need for Fourier Methods --$g5-2.$tWhat Are Your Choices and the Restrictions on FT-NMR? --$g1.$tNyquist Frequency --$g2.$tPulse Width --$g3.$tPulse Shape --$g4.$tResolution --$g5.$tData Registers --$g6.$tTruncation --$g7.$tDead Time --$g8.$tFolding Over --$g9.$tQuadrature Detection --$g10.$tPhasing --$g11.$tPulse Angle and Repetition Time --$g12.$tSpectral Enhancement by Exponential Multiplication --$g13.$tIntegration of NMR Spectra --$g5-3.$tAlternatives to the Fourier Transform --$g6.$tRelaxation and the Nuclear Overhauser Effect --$g6-1.$tSome General Considerations of T[subscript 2] Relaxation --$g6-2.$tGeneral Considerations of T[subscript 1] Relaxation --$g6-3.$tIntermolecular Mechanisms for T[subscript 1] Relaxation --$g1.$tRelaxation Induced by Unpaired Electrons --$g2.$tRelaxation Induced by Extramolecular Magnetic Nuclei --$g6-4.$tIntramolecular Mechanisms for T[subscript 1] Relaxation --$g1.$tQuadrupolar Relaxation --$g2.$tDipole-Dipole Relaxation --$g3.$tDecoupling of Nuclear Spins and the Nuclear Overhauser Effect --$g4.$tRelaxation by Chemical-Shift Anisotropy --$g5.$tSpin-Rotation Relaxation --$g6.$tScalar-Coupling Relaxation --$g7.$tPulse Experiments in One-Dimensional NMR Spectra --$g7-1.$tSelective Magnetization Transfer --$g7-2.$tInept Preparation for Inept --$g7-3.$tInept --$g7-4.$tPhase Cycling --$g7-5.$tRefocused INEPT --$g7-6.$tInept INEPT Summary --$g7-7.$tRole of J. Multiple-Quantum Coherences --$g7-8.$tDEPT and Its Variations --$g7-9.$tSoft Pulses and Their Uses --$g8.$tNMR Spectroscopy in Two Dimensions --$g8-1.$tWhat is a 2D Spectrum? --$g8-2.$tJ-Modulated 2D Spectra --$g8-3.$tSome Techniques and Considerations for Multidimensional Spectra --$g1.$tPhase Cycling --$g2.$tCross Relaxation --$g3.$tSpin Locking --$g4.$tHartmann-Hahn Condition and Cross Polarization --$g5.$tMagnetic Field Gradients --$g6.$tWaltz Decoupling --$g7.$tSuppression of Solvent Resonances --$g8.$tMultiple-Quantum Coherences Revisited --$g9.$tBloch-Siegert Shifts --$g8-4.$tHomonuclear Cosy Experiment --$g8-5.$tSome Capabilities of 2D Programs --$g1.$tHETCOR --$g2.$tNOESY --$g3.$tTOCSY --$g4.$tROESY --$g5.$tINADEQUATE --$g6.$tHMQC --$g7.$tProton Spectra without Spin-Spin Splittings --$g9.$tSome Thoughts on Spin-Spin Splitting --$g9-1.$tWhat are our Specific Objectives? --$g9-2.$tTwo-Nucleus System --$g9-3.$tClassification of NMR Spin Systems --$g9-4.$tMore Lines than Expected --$g9-5.$tPositive versus Negative J Values --$g9-6.$tUnexpected Splittings by Ostensibly Equivalent Nuclei --$g9-7.$tWhen What You See is Not Necessarily What is There --$g9-8.$tHow Can We Analyze Spin-Spin Splitting Patterns? --$g10.$tSome Thoughts about Chemical Shifts --$g10-1.$tWhy is the Range of Proton Chemical Shifts So Small? --$g10-2.$tElements of the Second-Order Paramagnetic Effect --$g10-3.$tSecond-Order Paramagnetic Effect and Nitrogen Shifts --$g10-4.$tSecond-Order Paramagnetic Effect and Proton Shifts --$g11.$tMeasurement of Rates by NMR --$g11-1.$tExample of the Determination of Rates by NMR --$g11-2.$tDerivations of Lineshapes in the Absence of Spin-Spin Splitting --$g11-3.$tMulti-Site Intermolecular Exchange Processes --$g11-4.$tLineshape Analysis to Determine Rates of Intramolecular Processes --$g11-5.$tLineshape Analysis for J-Coupled Systems --$g11-6.$tOther Methods of Determining Exchange Rates by NMR --$g1.$tCarr-Purcell Technique --$g2.$tSaturation Transfer --$g3.$tPulse Methods --$gAppendix 1.$tNMR Reference Books --$gAppendix 2.$tSimple Program for Calculating the Fourier Transform --$gAppendix 3.$tProgram for Simple Numerical Integration of the Bloch Equations --$gAppendix 4.$tQuantitative Approach to Spin-Spin Splitting.
650 0 $aFourier transform nuclear magnetic resonance spectroscopy.
650 7 $aFourier transform nuclear magnetic resonance spectroscopy.$2fast$0(OCoLC)fst00933408
650 07 $aFourier-Spektroskopie.$2swd
650 07 $aNMR-Spektroskopie.$2swd
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948 $hNO HOLDINGS IN P4A - 259 OTHER HOLDINGS